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1 article(s) from Wright, Andrew

3D printed fluidics with embedded analytic functionality for automated reaction optimisation

Andrew J. Capel,
Andrew Wright,
Matthew J. Harding,
George W. Weaver,
Yuqi Li,
Russell A. Harris,
Steve Edmondson,
Ruth D. Goodridge and
Steven D. R. Christie

Beilstein J. Org. Chem. 2017, 13, 111–119, doi:10.3762/bjoc.13.14

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Graphical Abstract

Scheme 1: The reaction of (R)-(−)-carvone (1) with semicarbazide to form the corresponding semicarbazone 2.

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Figure 1: CAD model of SL reactor design RD1 (left), RD1 with attached sprung clip (centre), commercially ava...

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Figure 2: Energy versus wavelength spectra comparing the amount of stray light being picked up by the detecto...

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Figure 3: Reactor set-up for carvone optimisation using RD1 as an inline spectroscopic flow cell. Reagents we...

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Figure 4: RD1 held in place within the DAD compartment of an Agilent 1100 HPLC.

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Figure 5: Optimisation plot for the SIMPLEX optimisation of semicarbazone 2. Optimum reaction conditions with...

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Figure 6: SLM reactor RD2 (left), CAD model of RD2 (right). External dimensions of RD2 are 100 (length) × 20 ...

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Figure 7: RD2 held in place within the thermostatted Agilent 1100 series column department.

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Figure 8: Optimisation plot for the SIMPLEX optimisation of semicarbazone 1. Optimum reaction conditions were...

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Scheme 2: The reaction of pentafluoropyridine (3) with 2-(methylamino)phenol (4) to form the corresponding fu...

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Figure 9: Optimisation plot for the SIMPLEX optimisation of the fused polycyclic heterocycle 5. Two optimal d...

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Figure 10: SLM reactor design RD3 (left), CAD model of RD3 (right). External dimensions of RD3 are 89 (length)...

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Figure 11: Optimisation plot for the SIMPLEX optimisation of semicarbazone 2. Optimum reaction conditions were...

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Published 18 Jan 2017

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